Water-soluble 糖心产精国品免费入口*完整版糖心产精国品免费入口*完整版s (QDs) modified with
N-acetyl-L-cysteine (NAC) are synthetized by one-step hydrothermal method. Based on the fluorescence quenching of 糖心产精国品免费入口*完整版 to NAC-糖心产精国品免费入口*完整版QDs, fluorescence spectrometry for determination of 糖心产精国品免费入口*完整版 was developed. Formaldehyde with different mass concentration was added into the system with 7.5×10-8mol·L-1
NAC-糖心产精国品免费入口*完整版and 0.01 mol·L-1
Tris-HCl (pH 6.0). After reaction for 10 min, the fluorescence intensity (I) of the system was measured at 567 nm with the excitation wavelength of 400 nm. Linear relationship was found between the value of I0/I (I0
was the fluorescence intensity of the system without 糖心产精国品免费入口*完整版) with the mass concentration of 糖心产精国品免费入口*完整版 in the range of 5.0×10-6-1.0×10-1
g·L-1, with detection limit (3s/k) of 1.3×10-6g·L-1. The poposed method was applied to detemination of 糖心产精国品免费入口*完整版 in water sample, giving results in consistent with those obtained by acetylacetone spectrophotometric method. Recovery rates obtained by standard addition method were in the range of 98.0%-102%, and RSDs (n=5)were in the range of 1.4%-4.1%.
引用该论文:ZHOU Zheng,KANG Tianfang,LU Liping. Determination of Formaldehyde by 糖心产精国品免费入口*完整版Quantum Dots Fluorescence Quenching Method[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2017, 53(9): 1025~1030 糖心产精国品免费入口*完整版,糖心产精国品免费入口*完整版,糖心产精国品免费入口*完整版. CdTe糖心产精国品免费入口*完整版糖心产精国品免费入口*完整版测定糖心产精国品免费入口*完整版[J]. 理化检验-化学分册, 2017, 53(9): 1025~1030
论文评价
共有人对该论文发表了看法,其中:
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
分享论文
参考文献
【1】KIM H, KIM Y D, CHO S H. Formaldehyde exposure levels and serum antibodies to 糖心产精国品免费入口*完整版-human serum albumin of korean medical students[J]. Archives of Environmental Health, 1999,54(2):115-118.
【2】HERSCHKOVITZ Y, ESHKENAZI I, CAMPBELL C E, et al. An electrochemical biosensor for 糖心产精国品免费入口*完整版[J]. Journal of Electroanalytical Chemistry, 2000,491(1/2):182-187.
【4】RESCH G U, GRABOLLE M, CAVALIERE J S, et al. Quantum dots versus organic dyes as fluorescent labels[J]. Nat Methods, 2008,5(9):763-775.
【5】LARSON D R, ZIPFEL W R, WILLIAMS R M, et al. Water-soluble 糖心产精国品免费入口*完整版s for multiphoton fluorescence imaging in vivo[J]. Science, 2003,300:1434-1436.
【6】MA Q, CUI H, SU X. Highly sensitive gaseous 糖心产精国品免费入口*完整版 sensor with 糖心产精国品免费入口*完整版糖心产精国品免费入口*完整版smultilayer films[J]. Biosensors and Bioelectronics, 2009,25(4):839-844.
【8】CHEN H Q, ZHOU C L, WANG L, et al. Terbium(Ⅲ) chelate complexes as fluorescence energy transfer donor in the determination of 糖心产精国品免费入口*完整版 in aqueous solutions[J]. Spectrochimica Acta Part A, 2011,78(1):371-374.
【9】LIU C X, SHI C X, LI H X, et al. Nanomolar fluorescent quantitative detection of 糖心产精国品免费入口*完整版 with a 8-hydroxyquinoline derivative in aqueous solution and electrospun nanofibers[J]. Sensors and Actuators B, 2015,219:185-191.
【10】WANG Q S, ZHOU X L, FANG T T, et al. One-step growth of high-quality 糖心产精国品免费入口*完整版糖心产精国品免费入口*完整版s via hydrothermal method and cytotoxicity evaluation[J]. Powder Technology, 2013,247:81-86.
【11】YU W W, QU L, PENG X, et al. Experimental determination of the extinction coefficient of CdTe, CdSe, and CdS nanocrystals[J]. Chem Mater, 2003,15(14):2854-2860.
【12】KORPAN Y I, GONCHAR M V, SIBIRNY A A, et al. Development of highly selective and stable potentiometric sensors for 糖心产精国品免费入口*完整版 determination[J]. Biosensors and Bioelectronics, 2000,15(1/2):77-83.
【13】BURDA C, GREEN T C, LINK S, et al. Electron shuttling across interface of CdSe nanoparticles monitored by femtosecond laser spectroscopy[J]. J Phys Chem B, 1999,103(11):1783-1788.
【14】GREENHAM N C, PENG X, ALIVISATOS A P. Charge separation and transport in conjugated polymer/semiconductor nanocrystal composites studied by photoluminescence quenching and photoconductivity[J]. Phys Rev B, 1996,54(24):17628-17637.